Major Research Facilities
Research facilities located in the Department of Chemical Engineering
include chemical and materials characterization and processing equipment,
a fully-staffed machine shop, and computer
server support.
Researchers also have access to several specialized
facilities, like CAMD (Center
for Advanced Microstructures and Devices) and PAL
(Polymer Analysis Laboratories).
Spectroscopic facilities consist of
a tunable femtosecond pump/probe laser, and a Nd:YAG laser with
all 4 harmonics (nanosecond laser); a Raman microprobe was recently
constructed. There are two Fourier transform infrared spectrometers
and four quadruple mass spectrometers. An energy dispensive X-ray
fluorescence analyzer is available in the department.
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| A VMC in the
Computer Numeric Controlled (CNC) Shop |
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The Department maintains an Electroscan E-3 Environmental
Scanning Electron Microscope as a multi-user facility available
to researchers around the campus and from outside industries. The
instrument can examine samples under vacuum or in the presence of
up to 20 Torr of a background gas (typically water vapor) with typical
resolution of 100 nm. Using a background gas reduces sample charging
problems, which means that insulating samples can be examined without
a separate coating step. It also allows users to examine wet samples
without dehydration (e.g., polymers and biological materials). Images
can be recorded digitally and transferred to users' files, where they
can be manipulated and displayed using standard image processing software.
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| Surface analysis
is an important characterization tool for a wide variety of
materials, ranging from heterogeneous catalysts to microelectronic
devices. |
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Processing facilities include, a CVD reactor,
catalytic reactors, extraction apparatus, an electrochemical impedance
analyser, potentiostats, thermogravimetric analyzers, a heat-flow
calorimeter, a BET surface area apparatus, several optical microscopes
of different types. A total carbon analyzer, a liquid scintillation
counter, gel-permeation and supercritical fluid chromatographs, an
HPLC, numerous LC's and GC's are used for environmental
and related studies. Incubators, shakers and culture cabinets--for
biochemical research. Rheological
and related properties of melts and solutions are studied on a constant
stress (concentric cylinder and cone and plate), capillary and torque
rheometers, a dynamic surface tensiometer, and a laser Doppler velocimeter.
Large-scale polymer processing equipment
includes two single and one twin screw extruders, an injection molder,
a high-sheer mixer, and a reaction injection molding machine.
We have several specially constructed high-pressure
facilities primarily used for equilibrium thermodynamics
and supercritical fluid extraction studies. In the
field of separations, there is a wet air stripping unit,
a distillation column and a bubble column, all pilot-scale.
Other equipment includes an apparatus to measure and analysis the
combustion of single droplets of hydrocarbon in the process ranges
from 3,000 to 4,000 psig and a facility which uses tomography and
image processing to measure and analysis the turbulent concentration
fields in stirred chemical reactors.
The Department houses its own Research and Development
Facility staffed by a master machinist and assistants.
Computational facilities include several Intel-based servers providing
File, Print, Web and e-mail services and about 120 personal computers
connected to the University network and through it to the Internet.
Each faculty and staff member has one of these computers in his
or her office and the rest are in the laboratories and student computer
labs.
The undergraduate student labs include teaching experiments utilizing
control systems from Nation Instruments, Fisher-Rosemont and Honeywell
TPS.
The department also has extensive experimental and diagnostic facilities
in the areas of environmental processes, catalytic and solid-state
surface characterization and materials processing.
This page was last modified on January 13, 2004 |